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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
65282-42-0
合成路线
（共 28 条）
154344-44-2
→
反应条件
65282-42-0
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: H2S / ethanol / pH 7.4 3: I2; NaHCO3 / ethanol 4: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 5: H2S / ethanol / pH 7.4 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-31-7
→
反应条件
65282-42-0
反应条件
1: H2S / ethanol / pH 7.4 2: I2; NaHCO3 / ethanol 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-46-4
→
反应条件
65282-42-0
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: H2S / ethanol / pH 7.4 3: I2; NaHCO3 / ethanol 4: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 5: H2S / ethanol / pH 7.4 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-34-0
→
反应条件
65282-42-0
反应条件
1: H2S / ethanol / pH 7.4 2: I2; NaHCO3 / ethanol 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
27916-10-5
→
反应条件
65282-42-0
反应条件
1: P4S10; pyridine 2: Hg(OAc)2 / acetic acid; CHCl3 View Scheme
参考文献
Salvetti, Raul; Martinetti, Giovanni; Ubiali, Daniela; Pregnolato, Massimo; Pagani, Giuseppe
Farmaco, 2003 , vol. 58, # 9 p. 995 - 998
154344-25-9
→
反应条件
65282-42-0
反应条件
1: I2; NaHCO3 / ethanol 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-28-2
→
反应条件
65282-42-0
反应条件
1: I2; NaHCO3 / ethanol 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
65282-42-0
→
反应条件
91859-66-4
反应条件
1: ethanol / Heating 2: I2; NaHCO3 / ethanol 3: Lawesson's reagent / toluene / 0.5 h / Heating 4: H2S / ethanol / pH 7.4 5: I2; NaHCO3 / ethanol 6: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 7: H2S / ethanol / pH 7.4 8: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 9: ethanol / Heating 10: I2; NaHCO3 / ethanol 11: Lawesson's reagent / toluene / 0.5 h / Heating 12: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 13: H2S / ethanol / pH 7.4 14: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 15: ethanol / Heating 16: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 17: ethanol / Heating 18: I2; NaHCO3 / ethanol 19: Lawesson's reagent / toluene / 0.5 h / Heating 20: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
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