反应条件
1: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 2: ethanol / Heating 3: I2; NaHCO3 / ethanol 4: Lawesson's reagent / toluene / 0.5 h / Heating 5: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 6: H2S / ethanol / pH 7.4 7: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 8: ethanol / Heating 9: I2; NaHCO3 / ethanol 10: Lawesson's reagent / toluene / 0.5 h / Heating 11: H2S / ethanol / pH 7.4 12: I2; NaHCO3 / ethanol 13: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 14: H2S / ethanol / pH 7.4 15: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 16: ethanol / Heating 17: I2; NaHCO3 / ethanol 18: Lawesson's reagent / toluene / 0.5 h / Heating 19: H2S / ethanol / pH 7.4 20: I2; NaHCO3 / ethanol 21: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 22: H2S / ethanol / pH 7.4 23: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 24: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 25: ethanol / Heating 26: P4S10 / xylene / 2 h / Heating 27: ethanol / Heating 28: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 29: I2; NaHCO3 / ethanol 30: Lawesson's reagent / toluene / 0.5 h / Heating 31: H2S / ethanol / pH 7.4 32: P4S10 / xylene / 2 h / Heating 33: ethanol / Heating 34: P4S10 / xylene / 2 h / Heating 35: ethanol / Heating 36: P4S10 / xylene / 2 h / Heating 37: ethanol / Heating 38: I2; NaHCO3 / ethanol 39: H2S / ethanol / pH 7.4 40: P4S10 / xylene / 2 h / Heating 41: ethanol / Heating 42: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
