1-(4-硝基苯基)乙醇合成路线 （共 41 条）
反应条件
thionyl chloride T=70 - 85°C;
参考文献
Russian Journal of General Chemistry, , vol. 83, # 10 p. 1859 - 1863
Zh. Obshch. Khim., , vol. 83, # 10 p. 1649 - 1653,5
反应条件
sol-gel entrapped pyridinium dichromate; hydrogen; sol-gel entrapped RhCl[P(C6H5)3]3 in 1,2-dichloro-ethane T=70°C; P=15960 Torr; 16 h; catalyst and pyridinium dichromate entrapped in separate sol-gel matrices;
参考文献
Gelman, Faina; Blum, Jochanan; Avnir, David
New Journal of Chemistry, 2003 , vol. 27, # 2 p. 205 - 207
反应条件
1: With oxygen; sodium hydride in tetrahydrofuran T=0 - 20°C; 30 h; 2: With hydrogenchloride in water
参考文献
Tetrahedron, , vol. 67, # 19 p. 3406 - 3411
参考文献
v. Braun; Bartsch
Chemische Berichte, 1913 , vol. 46, p. 3055
反应条件
1: PBr3
2: NaH / benzene; dimethylformamide
View Scheme
参考文献
Kelkar, S. V.; Joshi, G. S.; Kulkarni, G. H.; Mitra, R. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 68 - 70
反应条件
diethylamino-sulfur trifluoride; [C8mim][PF6]
T=20°C; 0.5 h;
参考文献
Das, Saibal; Chandrasekhar, Srivari; Yadav, Jhillu Singh; Gree, Rene
Tetrahedron Letters, 2007 , vol. 48, # 30 p. 5305 - 5307
反应条件
iodosylbenzene in acetonitrile
1.5 h; Heating;
参考文献
Ueno, Makoto; Nabana, Takahiro; Togo, Hideo
Journal of Organic Chemistry, 2003 , vol. 68, # 16 p. 6424 - 6426
反应条件
1: m-chloroperbenzoic acid; KBr / iodobenzene / acetonitrile / 1 h / 20 °C
2: 88 percent / m-chloroperbenzoic acid / iodobenzene / acetonitrile / 5 h / 50 °C
View Scheme
参考文献
Yamamoto, Yukiharu; Kawano, Yuhta; Toy, Patrick H.; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 22 p. 4680 - 4687
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
4.5 h; Reflux;
参考文献
Deshmukh, Swapnil S.; Huddar, Sameerana N.; Akamanchi, Krishnacharya G.
Synthetic Communications, 2009 , vol. 39, # 17 p. 3101 - 3110
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C
2: iodine / neat (no solvent) / 2 h / 85 °C
View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
