3,5-二甲氧基-4-(2-甲氧基乙氧基)苯甲醛合成路线 （共 3 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=150°C; 0.166667 h; Microwave irradiation;
参考文献
EXONHIT S.A.; LEBLOND, Bertrand; TAVERNE, Thierry; BEAUSOLEIL, Eric; CHAUVIGNAC, Cedric; CASAGRANDE, Anne-Sophie; DESIRE, Laurent
Patent: WO2011/151423 A1, 2011 ;
Location in patent: Page/Page column 93-94 ;
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=160°C; 0.333333 h; Microwave irradiationInert atmosphere;
参考文献
Wolfe, Amanda L.; Duncan, Katharine K.; Lajiness, James P.; Zhu, Kaicheng; Duerfeldt, Adam S.; Boger, Dale L.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 17 p. 6845 - 6857
反应条件
potassium carbonate in N,N-dimethyl-formamide
6 h; Heating;
参考文献
Buchtela; Liebenow; Vergin
Arzneimittel-Forschung/Drug Research, 1980 , vol. 30, # 2 p. 307 - 309
