6-叠氮基-6-脱氧-1,2-O-(1-甲基乙亚基)-alpha-D-呋喃葡萄糖合成路线 （共 8 条）
反应条件
sodium azide in N,N-dimethyl-formamide T=40°C; 15 h;
参考文献
Fernandez, Jose M. Garcia; Mellet, Carmen Ortiz; Maciejewski, Sylwester; Defaye, Jacques
Journal of the Chemical Society, Chemical Communications, 1996 , # 24 p. 2741 - 2742
反应条件
1: 91 percent / pyridine / 16 h / -15 °C 2: 92 percent / NaN3 / dimethylformamide / 20 h / 120 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 24 p. 2741 - 2742
反应条件
1: 93.2 percent / acetic acid / H2O / r.t., 6 h, 4 deg C, 12 h 2: 98 percent / pyridine / 12 h / -14 °C 3: 92 percent / NaN3 / dimethylformamide / 15 h / 40 °C View Scheme
参考文献
Tetrahedron, , vol. 45, # 1 p. 327 - 336
反应条件
1: 71 percent / sodium azide / dimethylformamide View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 15 p. 1413 - 1416
反应条件
hydrogenchloride 1.5 h; Ambient temperature;
参考文献
Liebigs Annalen der Chemie, , # 11 p. 1982 - 1993
反应条件
sodium azide; acetone
参考文献
Chemische Berichte, , vol. 92, p. 384,390
参考文献
Tetrahedron Letters, , vol. 22, # 15 p. 1413 - 1416
反应条件
trifluoroacetic acid in water
T=20°C; 1 h;
参考文献
Blanco, Jose L. Jimenez; Bootello, Purificacion; Mellet, Carmen Ortiz; Gallego, Ricardo Gutierrez; Fernandez, Jose M. Garcia
Chemical Communications (Cambridge, United Kingdom), 2004 , # 1 p. 92 - 93
