6,7-二甲氧基-2,2-二甲基-4-色满酮合成路线 （共 22 条）
反应条件
cesium fluoride in tetrahydrofuran T=125°C;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Tetrahedron, 2013 , vol. 69, # 13 p. 2789 - 2798
反应条件
potassium carbonate in acetone
参考文献
Alkaloida Vegyeszeti Gyar
Patent: US4866089 A1, 1989 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=40°C; 20 h;
参考文献
Teixidor, Pilar; Camps, Francisco; Messeguer, Angel
Heterocycles, 1988 , vol. 27, # 10 p. 2459 - 2466
反应条件
methanesulfonic acid; phosphorus pentoxide T=70°C; 0.75 h;
参考文献
Camps, F.; Coll, J.; Messeguer, A.; Pericas, M. A.; Ricart, S.; et al.
Synthesis, 1980 , # 9 p. 725 - 727
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide T=155 - 160°C; 1.5 h;
参考文献
Banerji, A.; Kalena, G.P.
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 159 - 166
反应条件
pyrrolidine in ethanol 12 h; Inert atmosphereReflux;
参考文献
Zhu, Mingyan; Kim, Myung Hee; Lee, Sanghee; Bae, Su Jung; Kim, Seong Hwan; Park, Seung Bum
Journal of Medicinal Chemistry, 2010 , vol. 53, # 24 p. 8760 - 8764
反应条件
hydrogenchloride in ethanol Heating;
参考文献
Roitman, James N.; Wollenweber, Eckhard
Phytochemistry (Elsevier), 1993 , vol. 33, # 4 p. 936 - 938
反应条件
1: 85 percent / Mg / benzene / 9 h / Heating 2: 22 percent / K2CO3 / hexane / 20 h / Irradiation 3: 98 percent / 10percent aq. NaOH / hexane / 4 h / Ambient temperature 4: 60 percent / methanol / 3 h 5: 85 percent / 25percent aq. NaOH, 20percent aq. Et4NOH / 1 h / 60 - 65 °C View Scheme
参考文献
Heterocycles, , vol. 32, # 6 p. 1159 - 1166
反应条件
1: 85 percent / Mg / benzene / 9 h / Heating 2: 22 percent / K2CO3 / hexane / 20 h / Irradiation 3: 98 percent / 10percent aq. NaOH / hexane / 4 h / Ambient temperature 4: 60 percent / methanol / 3 h 5: 85 percent / 25percent aq. NaOH, 20percent aq. Et4NOH / 1 h / 60 - 65 °C View Scheme
参考文献
Heterocycles, , vol. 32, # 6 p. 1159 - 1166
反应条件
1: 60 percent / methanol / 3 h 2: 85 percent / 25percent aq. NaOH, 20percent aq. Et4NOH / 1 h / 60 - 65 °C View Scheme
参考文献
Heterocycles, , vol. 32, # 6 p. 1159 - 1166
