2,3-二甲基吡嗪-n-氧化物合成路线 （共 6 条）
反应条件
1: 17 percent / POCl3 / 0.5 h / Heating 2: 46 percent / 90percent H2O2, maleic anhydride / CHCl3 / 1) room temp. 12 h 2) reflux, 5 h 3: 38 percent / POCl3 / 0.5 h / Heating View Scheme
参考文献
Watahiki, Hiroko; Tsutsui, Mayumi; Akita, Yasuo; Watanabe, Tokuhiro; Kurihara, Teruo
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 465 - 473
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
16 h;
参考文献
Leclerc, Jean-Philippe; Fagnou, Keith
Angewandte Chemie - International Edition, 2006 , vol. 45, # 46 p. 7781 - 7786
反应条件
sodium perborate in acetic acid
T=80°C; 5 h;
参考文献
Ohta, Akihiro; Ohta, Masakatsu
Synthesis, 1985 , # 2 p. 216 - 217
反应条件
trichlorophosphate
0.5 h; Heating;
参考文献
Watahiki, Hiroko; Tsutsui, Mayumi; Akita, Yasuo; Watanabe, Tokuhiro; Kurihara, Teruo
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 465 - 473
反应条件
trichlorophosphate
2 h; Heating / reflux;
参考文献
GLAXO GROUP LIMITED; DI FABIO, Romano
Patent: WO2012/89607 A1, 2012 ;
Location in patent: Page/Page column 48 ;
WO 2012/089607 A1
反应条件
trichlorophosphate
0.5 h; Heating;
参考文献
Watahiki, Hiroko; Tsutsui, Mayumi; Akita, Yasuo; Watanabe, Tokuhiro; Kurihara, Teruo
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 465 - 473
