3-苄基-6-溴-2-甲氧基喹啉合成路线 （共 6 条）
反应条件
in methanol 0.25 h; Heating;
参考文献
Pathak, Richa; Madapa, Sudharshan; Batra, Sanjay
Tetrahedron, 2007 , vol. 63, # 2 p. 451 - 460
反应条件
8 h; Heating / reflux;
参考文献
CHATTOPADHYAYA, Jyoti; UPADHAYAYA, Ram Shankar
Patent: WO2009/91324 A1, 2009 ;
Location in patent: Page/Page column 23 ;
WO 2009/091324 A1
反应条件
1: 97 percent / POCl3 / toluene / 0.5 h / 120 °C 2: 97 percent / methanol / 0.25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 451 - 460
反应条件
1: 79 percent / TFA / 60 °C 2: 100 percent / K2CO3 / acetone / 0.25 h / 60 °C 3: 97 percent / POCl3 / toluene / 0.5 h / 120 °C 4: 97 percent / methanol / 0.25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 451 - 460
反应条件
1: pyridine / CH2Cl2 / 3 h / 20 °C 2: 75 percent / DABCO / tetrahydrofuran; H2O / 3 h / 20 °C 3: 79 percent / TFA / 60 °C 4: 100 percent / K2CO3 / acetone / 0.25 h / 60 °C 5: 97 percent / POCl3 / toluene / 0.5 h / 120 °C 6: 97 percent / methanol / 0.25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 451 - 460
反应条件
1: 75 percent / DABCO / tetrahydrofuran; H2O / 3 h / 20 °C 2: 79 percent / TFA / 60 °C 3: 100 percent / K2CO3 / acetone / 0.25 h / 60 °C 4: 97 percent / POCl3 / toluene / 0.5 h / 120 °C 5: 97 percent / methanol / 0.25 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 451 - 460
