2,2,2,4'-四氟苯乙酮合成路线 （共 25 条）
反应条件
benzo[1,3,2]dioxaborole in dichloromethane T=-78°C;
参考文献
APPLERA CORPORATION
Patent: WO2006/102535 A2, 2006 ;
Location in patent: Page/Page column 68 ;
WO 2006/102535 A2
反应条件
(-)-(S)-BINAL-H in tetrahydrofuran T=0°C; 3 h;
参考文献
Chong, J. Michael; Mar, Eduardo K.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 893 - 896
反应条件
1: Nafion-H SAC-13 / toluene / 24 h / 185 °C 2: hydrogenchloride; water / diethyl ether / 24 h / 20 °C View Scheme
参考文献
Prakash, G.K. Surya; Glinton, Kevin E.; Panja, Chiradeep; Gurung, Laxman; Battamack, Patrice T.; Toeroek, Bela; Mathew, Thomas; Olah, George A.
Tetrahedron Letters, 2012 , vol. 53, # 6 p. 607 - 611
反应条件
1: Et3N / dimethylsulfoxide / 0.5 h
2: aq. NaOH / dimethylformamide / 2 h
View Scheme
参考文献
Shinozuka, Tsuyoshi; Nakao, Akira; Saito, Keiji; Naito, Satoru
Chemistry Letters, 2006 , vol. 35, # 10 p. 1090 - 1091
反应条件
sodium carbonate in dimethyl sulfoxide
参考文献
Science Union et Cie
Patent: US4288453 A1, 1981 ;
