alpha-环丙基-4-甲氧基苄醇合成路线 （共 6 条）
反应条件
dipotassium peroxodisulfate; acetonitrile in water T=25°C; pH=9.5; 0.00833333 h; Irradiation;
参考文献
Bietti, Massimo; Fiorentini, Simone; Pato, Iria Perez; Salamone, Michela
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3167 - 3175
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C 1.2: 8 h / 20 °C 2.1: triethylsilane; anhydrous iron chloride / dichloromethane / 1.5 h / 20 °C View Scheme
参考文献
Fan, Xiaohui; Cui, Xiao-Meng; Guan, Yong-Hong; Fu, Lin-An; Lv, Hao; Guo, Kun; Zhu, Hong-Bo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 498 - 501
反应条件
titanium(IV) isopropylate; (1R,2S)-N-(O,O-dimethylthiophosphoryl)norephedrine in toluene
T=-30°C; 3 h;
参考文献
Shibata, Takanori; Tabira, Hayami; Soai, Kenso
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 2 p. 177 - 178
反应条件
lithium aluminium tetrahydride in diethyl ether
2 h;
参考文献
Matveeva; Kvasha; Kurts
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 1 p. 17 - 20
反应条件
in tetrahydrofuran
T=20°C; 3 h; Inert atmosphere;
参考文献
Qi, Wenke; Wang, Peipei; Fan, Liyuan; Zhang, Songlin
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 5918 - 5924
反应条件
magnesium
1.) THF, 0 deg C, 60 min, 2.) 25 deg C, 16 h; Yield given. Multistep reaction;
参考文献
McCormick, J. P.; Fitterman, Alan S.; Barton, Donald L.
Journal of Organic Chemistry, 1981 , vol. 46, # 23 p. 4708 - 4712
