反应条件
1: 40 percent / potassium metal, NH3 (liquid) / 1) -33 deg C, 30 min, 2) r.t., 3 h
2: 98 percent / potassium t-butoxide / dimethylsulfoxide / 6 h / Ambient temperature
3: 10 percent / POCl3 / CHCl3 / 4 h / Heating
4: 90 percent / hydrogen / 5percent Pd/C / ethanol / 5 h / 1034.3 Torr / Ambient temperature
5: 1) potassium t-butoxide, O2, 2) gl. acetic acid, zinc dust / 1) t-butanol, 35 deg C, 5 min, 2) 6 h, r.t.
6: 70 percent / aluminium chloride, sodium chloride / 0.08 h / 180 °C
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Sathaye, K. M.; Jaweed, S. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 697 - 702
