2,4,6-三异丙基苯磺酰氯合成路线 （共 18 条）
反应条件
tetrabutylammomium bromide; sodium carbonate in dichloromethane T=20°C; 12 h;
参考文献
Yamada, Kenji; Hattori, Yusaku; Inde, Takeshi; Kanamori, Takashi; Ohkubo, Akihiro; Seio, Kohji; Sekine, Mitsuo
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 3 p. 776 - 778
反应条件
chloro-trimethyl-silane; ethylene dibromide; acetyl chloride; zinc in ethyl acetate
参考文献
Chemla, Fabrice
Synlett, 1998 , # 8 p. 894 - 896
反应条件
(i) LiAlH4, Et2O, (ii) I2, benzene; Multistep reaction;
参考文献
Adlington, Robert M.; Barrett, Anthony G. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1076 - 1079
反应条件
1: 85 percent / Zn, HCl
2: Cl2 / CCl4 / 0 °C
View Scheme
参考文献
Garratt, Dennis G.; Beaulieu, Pierre L.
Canadian Journal of Chemistry, 1980 , vol. 58, # 24 p. 2738 - 2744
参考文献
Guthrie, R. D. (Gus); Thang, San
Australian Journal of Chemistry, 1987 , vol. 40, # 12 p. 2133 - 2136
参考文献
Pearson,D.E. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 867 - 869
反应条件
1: ammonium hydroxide / chloroform / 2 h / 20 °C / |Inert atmosphere
2: triethylamine; titanium tetrachloride / dichloromethane / 1 h / 0 °C / |Inert atmosphere
View Scheme
参考文献
Han, Zhiqiang; Yang, Wenguo; Tan, Choon-Hong; Jiang, Zhiyong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1505 - 1511
反应条件
1: Et3N / dimethylformamide
2: aq. HClO4 / dioxane
View Scheme
参考文献
Tamura; Minamikawa; Sumoto; Fujii; Ikeda
The Journal of organic chemistry, 1973 , vol. 38, # 6 p. 1239 - 1241
