3,3-二甲基螺[环丙烷-1,1'-[1H]茚]-2-羧酸乙酯合成路线 （共 4 条）
反应条件
T=60 - 70°C; P=1 Torr;
参考文献
Galin, F. Z.; Ignatyuk, V. K.; Lakeev, S. N.; Rakhimov, R. G.; Sultanova, V. S.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 1.1 p. 92 - 98
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 1 p. 103 - 111
反应条件
rhodium (II) acetate
Ambient temperature;
参考文献
Galin, F. Z.; Ignatyuk, V. K.; Lakeev, S. N.; Rakhimov, R. G.; Sultanova, V. S.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 1.1 p. 92 - 98
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 1 p. 103 - 111
反应条件
1: 82 percent / CH3ONa / 55 - 70 °C
2: 11 percent / rhodium acetate / Ambient temperature
View Scheme
参考文献
Galin, F. Z.; Ignatyuk, V. K.; Lakeev, S. N.; Rakhimov, R. G.; Sultanova, V. S.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 1.1 p. 92 - 98
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 1 p. 103 - 111
反应条件
1: aq. potassium hydroxide / ethanol / 2 h / 60 °C
2: thionyl chloride / benzene / 1.) 25 deg C, 12 h, 2.) reflux, 20 min
View Scheme
参考文献
Tolstikov, G. A.; Galin, F. Z.; Ignatyuk, V. K.; Lakeev, S. N.; Berg, A. A.; et al.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 6.1 p. 1090 - 1100
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 6 p. 1209 - 1222
