反应条件
1: dicyclo-hexylphosphine With N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran; hexane
T=25°C; 0.5 h;
2: 1,5-dihydro-benzo[e][1,3,2]dioxathiepine 3,3-dioxide in tetrahydrofuran; hexane
T=-78 - 20°C; 1 h;
3: lithium diphenylphosphinide in tetrahydrofuran; hexane
T=60°C; 3 h;
参考文献
Leone, Antonella; Consiglio, Giambattista
Helvetica Chimica Acta, 2005 , vol. 88, # 2 p. 210 - 215
