2-(6-溴己基)-丙二酸二乙酯合成路线 （共 16 条）
参考文献
Salmon-Legagneur; Neveu
Bulletin de la Societe Chimique de France, 1956 , p. 1345,1350
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: NH3 / tetrahydrofuran / 15 h
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: 58 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
3: H2 / PtO2 / diethyl ether
4: pyridine / 0 °C
5: NaI / acetone / 2 h / Heating
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
3: H2 / PtO2 / diethyl ether
4: pyridine / 0 °C
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
3: H2 / PtO2 / diethyl ether
4: pyridine / 0 °C
5: NaI / acetone / 2 h / Heating
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C
2: NH3 / tetrahydrofuran / 15 h
3: diethyl ether
View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
