N-丁基-N-(2-甲氧基苯基)胺合成路线 (共 18 条)
反应条件
triethylamine in toluene
T=0 - 20°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
Qian, Xin; Yu, Zailu; Auffrant, Audrey; Gosmini, Corinne
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6225 - 6229
反应条件
copper(l) iodide; potassium tert-butylate; water in dimethyl sulfoxide
T=160°C; 8 h; Inert atmosphere;
参考文献
Zheng; Xu; Shi; Ren; Lu; Zhou
Asian Journal of Chemistry, 2013 , vol. 25, # 2 p. 1117 - 1122
反应条件
copper diacetate; triethylamine in dichloromethane
Ambient temperature;
参考文献
Cundy, Darren J.; Forsyth, Stewart A.
Tetrahedron Letters, 1998 , vol. 39, # 43 p. 7979 - 7982
反应条件
tris(triphenylphosphine)ruthenium(II) chloride
T=180°C; 5 h;
参考文献
Watanabe, Yoshihisa; Tsuji, Yasushi; Ige, Hitoshi; Ohsugi, Yukihiro; Ohta, Tetsuo
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3359 - 3363
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) 0 deg C, 30 min; room temp., 1 h, 2.) reflux, overnight; Yield given;
参考文献
Hoeve, Wolter ten; Kruse, Chris, G.; Luteyn, Jan M.; Thiecke, Janet R. G.; Wynberg, Hans
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5101 - 5106
反应条件
in water
2 h; Heating;
参考文献
Giuliani; Lembo; Sasso; Sorrentino; Silipo; Vittoria
Farmaco, Edizione Scientifica, 1983 , vol. 38, # 11 p. 847 - 864
反应条件
1.1: cobalt(II) dibromide; trifluoroacetic acid; 3-chloroprop-1-ene / acetonitrile / 0.05 h / 20 °C
1.2: 20 °C
2.1: triethylamine / toluene / 2 h / 0 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Qian, Xin; Yu, Zailu; Auffrant, Audrey; Gosmini, Corinne
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6225 - 6229
参考文献
de Beer et al.
Journal of Pharmacology and Experimental Therapeutics, 1936 , vol. 57, p. 19,22