反应条件
1: 1) BuLi / 1) DMF, hexane, -50 deg C, 2h, 2) -50 to -60 deg C, 2h
2: 86 percent / LiAlH4 / diethyl ether / 0.5 h / -40 °C
View Scheme
参考文献
Tsuboi, Sadao; Ishii, Naomi; Sakai, Takashi; Tari, Isao; Utaka, Masanori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 7 p. 1888 - 1893
