1-(4-氯苯基)-3-(2-羟基苯基)丙烷-1,3-二酮合成路线 （共 10 条）
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 2 h; Further byproducts given;
参考文献
Nishinaga, Akira; Maruyama, Kazushige; Ando, Hiroyuki; Sato, Ryoji; Mashino, Takahiro; Inada, Akira; Nakanishi, Tsutomu
Tetrahedron Letters, 1990 , vol. 31, # 22 p. 3171 - 3174
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 2 h; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 31, # 22 p. 3171 - 3174
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen T=60°C; P=760 Torr; 2 h; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 31, # 22 p. 3171 - 3174
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
1 h; Ambient temperature;
参考文献
Nishinaga; Ando; Maruyama; Mashino
Synthesis, 1992 , # 9 p. 839 - 841
反应条件
1: pyridine / 25 °C / Cooling with ice
2: potassium tert-butylate / N,N-dimethyl-formamide / 1.17 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Krayushkin, Mikhail M.; Levchenko, Konstantin S.; Yarovenko, Vladimir N.; Christoforova, Ludmila V.; Barachevsky, Valery A.; Puankov, Yury A.; Valova, Tatyana M.; Kobeleva, Olga I.; Lyssenko
New Journal of Chemistry, 2009 , vol. 33, # 11 p. 2267 - 2277
反应条件
potassium carbonate in acetone
Reflux;
参考文献
Zheng, Xing; Zhao, Fei Fei; Liu, Yun Mei; Yao, Xu; Zheng, Zi Tong; Luo, Xing; Liao, Duan Fang
Medicinal Chemistry, 2010 , vol. 6, # 1 p. 6 - 8
参考文献
Baker et al.
Journal of the Chemical Society, 1952 , p. 1294,1301
Journal of the Chemical Society, 1954 , p. 998,1000
反应条件
bis(trichloromethyl) carbonate; N,N-dimethyl-formamide in 1,2-dichloro-ethane
T=0 - 20°C; 2 h;
参考文献
Zhu, Xingyi; Li, Zhenhua; Shu, Qiangfeng; Zhou, Chenfeng; Su, Weike
Synthetic Communications, 2009 , vol. 39, # 23 p. 4199 - 4211
反应条件
lt;Co(III)(N1,N7-4-azaheptamethylenebis(salicylideneiminato))gt;hydroxide; oxygen
T=60°C; P=760 Torr; 2 h; Further byproducts given;
参考文献
Nishinaga, Akira; Maruyama, Kazushige; Ando, Hiroyuki; Sato, Ryoji; Mashino, Takahiro; Inada, Akira; Nakanishi, Tsutomu
Tetrahedron Letters, 1990 , vol. 31, # 22 p. 3171 - 3174
反应条件
thiophosphoryl trichloride; water; triethylamine
T=30 - 80°C; 0.333333 h;
参考文献
Vimal, Manorama; Pathak, Uma; Pandey, Lokesh Kumar; Suryanarayana, Malladi V. S.
Synthesis, 2011 , # 1 p. 30 - 32
