三[2-(甲基氨基)乙基]胺合成路线 （共 14 条）
反应条件
potassium tert-butylate in acetonitrile 1) 1h, RT, 2) 1 h, RT;
参考文献
Tetrahedron Letters, , vol. 34, # 18 p. 2903 - 2904
反应条件
1: 82 percent / ClP(NMe2)2, Et3N / CH2Cl2 / 1 h / Ambient temperature 2: 53 percent / NaOH / 200 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 9 p. 3478 - 3479
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 41, p. 21 - 30
反应条件
1: 93 percent / toluene / 7 h / Heating 2: 87 percent / N-chlorosuccinimide / CH2Cl2 / -50 - -10 °C 3: benzene-d6 / Ambient temperature 4: 70 percent / CCl4 / 10 h / Ambient temperature 5: 26 percent / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Wan, Yanjian; Verkade, John G.
Journal of the American Chemical Society, 1995 , vol. 117, # 1 p. 141 - 156
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Turnbull, W Bruce; Kalovidouris, Stacey A; Stoddart, J Fraser
Chemistry (Weinheim an der Bergstrasse, Germany), 2002 , vol. 8, # 13 p. 2988 - 3000
反应条件
1: in water; toluene
2: With lithium aluminium tetrahydride in tetrahydrofuran; water; toluene
参考文献
Comby, Steve; Imbert, Daniel; Vandevyver, Caroline; Buenzli, Jean-Claude G.
Chemistry - A European Journal, 2007 , vol. 13, # 3 p. 936 - 944
反应条件
1: 82 percent / KOH / benzene; H2O / 18 h / 20 °C
2: LiAlH4 / tetrahydrofuran / 18 h / Heating
View Scheme
参考文献
Torti, Suzy V.; Ma, Rong; Venditto, Vincent J.; Torti, Frank M.; Planalp, Roy P.; Brechbiel, Martin W.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 21 p. 5961 - 5967
反应条件
in benzene-d6
in an NMR tube for 0.5 h;; NMR;;
参考文献
Wan, Yanjian; Verkade, John G.
Inorganic Chemistry, 1993 , vol. 32, p. 79 - 81
反应条件
1: (NH4)2SO4
2: benzene-d6
View Scheme
参考文献
Wan, Yanjian; Verkade, John G.
Inorganic Chemistry, 1993 , vol. 32, p. 79 - 81
反应条件
1: benzene-d6
2: benzene-d6
View Scheme
参考文献
Wan, Yanjian; Verkade, John G.
Inorganic Chemistry, 1993 , vol. 32, p. 79 - 81
