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kieselgel; ozone T=-78°C;

in tetrahydrofuran under Ar, conventional Schlenk techniques; 10 equiv. of ligand added to soln. of Ru complex in THF; stirred under H2 (1 atm) at room temp. for ca. 3 h; filtered; evapd. to dryness; detd. by (1)H NMR spectroscopy;