2-(3-甲氧基苯甲酰胺基)乙酰氧肟酸合成路线 (共 3 条)
反应条件
potassium hydroxide; hydroxylamine hydrochloride in methanol
Ambient temperature; Yield given;
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: K2CO3 / H2O; toluene / -5 - 5 °C
2: NH2OH*HCl, KOH / methanol / Ambient temperature
View Scheme
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: SOCl2, DMF / toluene / 0.5 h / 60 - 70 °C
2: K2CO3 / H2O; toluene / -5 - 5 °C
3: NH2OH*HCl, KOH / methanol / Ambient temperature
View Scheme
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051