叔丁氧甲酰基-N-ε-二甲基-L-赖氨酸合成路线 (共 2 条)
反应条件
hydrogen; palladium 10 on activated carbon in water T=25°C; P=2585.81 Torr; 96 h;
参考文献
Schering Corporation
Patent: US2007/15774 A1, 2007 ;
Location in patent: Page/Page column 223-224 ;
反应条件
1: N-ethyl-N,N-diisopropylamine / acetonitrile; methanol / 1 h / 20 °C 2: sodium hydroxide / water; methanol / 1 h / 20 °C 3: dichloromethane / 3 h / 20 °C 4: sodium carbonate / water; 1,4-dioxane / 8 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 35 p. 14310 - 14313