3,4-二氯-5-硝基三氟甲苯合成路线 (共 5 条)
反应条件
sulfuric acid; nitric acid
参考文献
Rohm and Haas Company
Patent: US4046798 A1, 1977 ;
反应条件
sulfuric acid; nitric acid 120 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 4, # 2 p. 247 - 253
反应条件
potassium fluoride; anhydrous tetramethylammonium chloride
参考文献
Occidental Chemical Corporation
Patent: US4582948 A1, 1986 ;
反应条件
1: (i) aq. KOH, (ii) /BRN= 1983155/, sulfolane
2: H2 / PtO2 / ethanol
3: (i) NaNO2, aq. HCl, (ii) CuCl
View Scheme
参考文献
Rohm and Haas
Patent: CH567359DE2311638 , 1975 ;
Chem.Abstr., 1974 , vol. 80, # 3253
参考文献
Rohm and Haas Company
Patent: US4419122 A1, 1983 ;