反应条件
Na; MeOH in acetonitrile simultaneous addn. of solns. of Ni-complex and Na/MeOH to boiling MeCN (over 4 h), refluxing (24 h, pptn.), cooling to room temp.; filtration, volume reduction, repeated chromy. (Al2O3,MeCN), EtOH addn., crystn. (12 h, freezer), washing (EtOH), drying (vac.); elem. anal.;
参考文献
Alcock, Nathaniel W.; Padolik, Peter A.; Pike, Graham A.; Kojima, Masaaki; Cairns, Colin J.; Busch, Daryle H.
Inorganic Chemistry, 1990 , vol. 29 - 14, p. 2599 - 2607
