2-(三氟甲基)苯并呋喃合成路线 (共 14 条)
反应条件
tert.-butylhydroperoxide; copper(l) chloride in methanol; dichloromethane; water
T=0 - 20°C; 12 h;
参考文献
Ye, Yingda; Kuenzi, Stefan A.; Sanford, Melanie S.
Organic Letters, 2012 , vol. 14, # 19 p. 4979 - 4981,3
Title/Abstract Full Text Show Details
Ye, Yingda; Kuenzi, Stefan A.; Sanford, Melanie S.
Organic Letters, 2012 , vol. 14, # 19 p. 4979 - 4981
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate in diethylene glycol dimethyl ether
T=35°C; 14 h; Inert atmosphere;
参考文献
Liu, Tianfei; Shen, Qilong
Organic Letters, 2011 , vol. 13, # 9 p. 2342 - 2345
反应条件
potassium fluoride; potassium phosphate; 1,10-phenanthroline; copper (I) trifluoromethane sulfonate benzene; silver carbonate in N,N-dimethyl-formamide
T=45°C; Inert atmosphere;
参考文献
Chu, Lingling; Qing, Feng-Ling
Organic Letters, 2010 , vol. 12, # 21 p. 5060 - 5063
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=20°C; 27 h;
参考文献
Zhou, Hua; Niu, Jia-Jia; Xu, Jing-Wei; Hu, Shao-Jing
Synthetic Communications, 2009 , vol. 39, # 4 p. 716 - 732
反应条件
copper; sodium hydrogencarbonate in N,N-dimethyl-formamide
T=50°C; 11 h; Sealed tube;
参考文献
Zhang, Cheng-Pan; Cai, Ji; Zhou, Chang-Bing; Wang, Xiao-Ping; Zheng, Xing; Gu, Yu-Cheng; Xiao, Ji-Chang
Chemical Communications, 2011 , vol. 47, # 33 p. 9516 - 9518
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; anhydrous copper acetate; potassium carbonate in N,N-dimethyl-formamide
T=40°C; 12 h; Inert atmosphere26 W fluorescent light bulbs;
参考文献
Ye, Yingda; Sanford, Melanie S.
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9034 - 9037
反应条件
tert.-butylhydroperoxide; copper(l) chloride in methanol; dichloromethane; water
T=0 - 20°C; 12 h;
参考文献
Presset, Marc; Oehlrich, Daniel; Rombouts, Frederik; Molander, Gary A.
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12837 - 12843
反应条件
in 1,2,2-trifluoro-trichloroethane
T=60°C;
参考文献
Sawada, Hideo; Nakayama, Masaharu; Yoshida, Masato; Yoshida, Tatsuro; Kamigata, Nobumasa
Journal of Fluorine Chemistry, 1990 , vol. 46, # 3 p. 423 - 431
反应条件
1,10-phenanthroline; lithium hydroxide hydrate; CuTC in dichloromethane
T=45°C; Inert atmosphere;
参考文献
Liu, Tianfei; Shao, Xinxin; Wu, Yaming; Shen, Qilong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 540 - 543
反应条件
1H-imidazole; 2,4,6-trimethyl-pyridine; tert.-butylhydroperoxide; copper diacetate; ammonium chloride in dichloromethane; water
T=20°C; 6 h;
参考文献
Li, Yang; Wu, Lipeng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2013 , vol. 49, # 26 p. 2628 - 2630