二乙基2,2'-联吡啶-6,6'-二羧酸酯合成路线 (共 2 条)
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride
T=70°C; Carboxylation; esterification; P=760.051 Torr; 12 h;
参考文献
El-Ghayoury; Ziessel
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7757 - 7763
反应条件
sulfuric acid
T=20°C; RefluxInert atmosphere;
参考文献
Bozoklu, Guelay; Marchal, Claire; Gateau, Christelle; Pecaut, Jacques; Imbert, Daniel; Mazzanti, Marinella
Chemistry - A European Journal, 2010 , vol. 16, # 21 p. 6159 - 6163