2-甲基-5,6-二氢-1,4-氧硫杂环己二烯-3-甲酸合成路线 （共 6 条）
反应条件
sulfuryl dichloride in tetrachloromethane; dichloromethane
T=-14°C; 3 h;
参考文献
Nevalainen, Vesa; Pohjala, Esko
Journal of Chemical Research, Miniprint, 1988 , # 6 p. 1401 - 1421
反应条件
sodium hydroxide in ethanol
Heating; Yield given;
参考文献
Nevalainen, Vesa; Pohjala, Esko; Maelkoenen, Pentti; Hukkanen, Heikki
Acta Chemica Scandinavica, 1990 , vol. 44, # 6 p. 591 - 602
Title/Abstract Full Text Show Details
Nevalainen, Vesa; Pohjala, Esko
Journal of Chemical Research, Miniprint, 1988 , # 6 p. 1401 - 1421
反应条件
1: 1) SO2Cl2, 2) NEt3 / 1) CH2Cl2, CCl4, -10 deg C, 3 h, 2a) CH2Cl2, up to r.t., 2b) reflux, 2 h
2: aq.NaOH / ethanol / Heating
View Scheme
参考文献
Nevalainen, Vesa; Pohjala, Esko
Journal of Chemical Research, Miniprint, 1988 , # 6 p. 1401 - 1421
反应条件
sodium hydroxide in ethanol
Heating; Yield given;
参考文献
Nevalainen, Vesa; Pohjala, Esko; Maelkoenen, Pentti; Hukkanen, Heikki
Acta Chemica Scandinavica, 1990 , vol. 44, # 6 p. 591 - 602
反应条件
1: NEt3 / acetone / 0.5 h / 0 °C
2: sodium azide / acetone; H2O / 1 h / Ambient temperature
View Scheme
参考文献
Eckstein, Zygmunt; Rafa, Jadwiga; Rusek, Dorota
Polish Journal of Chemistry, 1982 , vol. 56, # 4-6 p. 841 - 847
反应条件
1: NEt3 / acetone / 0.5 h / 0 °C
2: NaHS / dimethylformamide / 0.5 h
View Scheme
参考文献
Eckstein, Zygmunt; Rafa, Jadwiga; Rusek, Dorota
Polish Journal of Chemistry, 1982 , vol. 56, # 4-6 p. 841 - 847
