Budke, Brian; Kalin, Jay H.; Pawlowski, Michal; Zelivianskaia, Anna S.; Wu, Megan; Kozikowski, Alan P.; Connell, Philip P.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 1 p. 254 - 263
1: sodium acetate / acetic anhydride / 0.5 h / 20 - 100 °C
2: thionyl chloride; pyridine / 1.25 h / 0 °C / |Reflux
View Scheme
参考文献
Budke, Brian; Kalin, Jay H.; Pawlowski, Michal; Zelivianskaia, Anna S.; Wu, Megan; Kozikowski, Alan P.; Connell, Philip P.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 1 p. 254 - 263
1: diethyl ether / 2 h / 20 °C
2: sodium acetate / acetic anhydride / 0.5 h / 20 - 100 °C
3: thionyl chloride; pyridine / 1.25 h / 0 °C / |Reflux
View Scheme
参考文献
Budke, Brian; Kalin, Jay H.; Pawlowski, Michal; Zelivianskaia, Anna S.; Wu, Megan; Kozikowski, Alan P.; Connell, Philip P.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 1 p. 254 - 263
