5-溴甲基-2,1,3-苯并噻重氮合成路线 （共 7 条）
参考文献
Bulletin of the Chemical Society of Japan, , vol. 32, p. 551
反应条件
N-bromosuccinmide in chloroform
参考文献
US6593335 B1, ;
US 6593335 B1
参考文献
Abbott Laboratories
Patent: US6593335 B1, 2003 ;
US 6593335 B1
反应条件
1: 2.66 g / CaCO3; water / dioxane / 3 h / Heating 2: 1.9 g / MnO2 / CHCl3 / 20 °C View Scheme
参考文献
Slavachevskaya,N.M. et al.
Pharmaceutical Chemistry Journal, 1979 , vol. 13, # 6 p. 591 - 598
Khimiko-Farmatsevticheskii Zhurnal, 1979 , vol. 13, # 6 p. 33 - 41
反应条件
2: aqueous acetic acid; hexamethylenetetramine 3: AgNO3; aqueous NaOH View Scheme
参考文献
Sekikawa
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 551
反应条件
2: piperidine / methanol
3: aq. HCl / CHCl3
4: (i) MeOH, (ii) H2S
View Scheme
参考文献
Slavachevskaya,N.M. et al.
Pharmaceutical Chemistry Journal, 1979 , vol. 13, # 6 p. 591 - 598
Khimiko-Farmatsevticheskii Zhurnal, 1979 , vol. 13, # 6 p. 33 - 41
反应条件
1: CHCl3 / Heating
2: HCl / ethanol
View Scheme
参考文献
Sharma,K.S.; Singh,V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1979 , vol. 18B, p. 556 - 557
