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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
65859-90-7
合成路线
（共 20 条）
65859-90-7
→
反应条件
36092-42-9
DL-苄基琥珀酸
反应条件
1: H2 / 10 percent Pd/C / ethyl acetate / 6 h / 20 °C / 2068.59 Torr 2: 75 percent / aq. NaOH / ethanol / 5 h / Heating View Scheme
参考文献
Ballini, Roberto; Bosica, Giovanna; Fiorini, Dennis; Righi, Paolo
Synthesis, 2002 , # 5 p. 681 - 685
65859-90-7
→
反应条件
35262-43-2
DL-苄基琥珀酸二甲酯
反应条件
hydrogen; triethylamine; {RuHCl((R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2} in tetrahydrofuran; ethanol T=35°C; P=1520 Torr; 48 h; Ru2Cl4-bis<(R)-(+)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl;
参考文献
Kawano, Hiroyuki; Ikariya, Takao; Ishii, Youichi; Saburi, Masahiko; Yoshikawa, Sadao; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1571 - 1575
65859-90-7
+
100-52-7
苯甲醛
→
反应条件
121851-40-9
反应条件
1: With lithium methanolate in methanol Stobbe condensation; 36 h; Heating; 2: With hydrogenchloride pH=1; Further stages.;
参考文献
Bilenko, Vitaliy; Jiao, Haijun; Spannenberg, Anke; Fischer, Christine; Reinke, Helmut; Koesters, Jutta; Komarov, Igor; Boerner, Armin
European Journal of Organic Chemistry, 2007 , # 5 p. 758 - 767
108-86-1
溴代苯
+
617-52-7
衣康酸二甲酯
→
反应条件
65859-90-7
反应条件
α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide; 1-(4-hydroxyphenyl)ethanone oxime in N,N-dimethyl acetamide; water Heck reaction; 14 h; Heating;
参考文献
Botella, Luis; Najera, Carmen
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4360 - 4369
100-52-7
苯甲醛
+
624-48-6
马来酸二甲酯
→
反应条件
65859-90-7
反应条件
tris(4-methoxyphenyl)-phosphine in acetonitrile T=80°C; 36 h; stereoselective reaction;
参考文献
Jiang, Huanfeng; Wang, Wei; Liu, Weibing; Qiao, Chunli
Chinese Journal of Chemistry, 2010 , vol. 28, # 2 p. 263 - 268
591-50-4
碘苯
+
617-52-7
衣康酸二甲酯
→
反应条件
65859-90-7
反应条件
α-cyclohexylcyclohexanemethanamine; 1-(4-hydroxyphenyl)ethanone oxime in water Heck reaction; 14 h; Heating;
参考文献
Botella, Luis; Najera, Carmen
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4360 - 4369
100-52-7
苯甲醛
+
106-65-0
丁二酸二甲酯
→
反应条件
65859-90-7
反应条件
1: With potassium tert-butylate in tert-butyl alcohol T=25°C; Stobbe condensation; 0.5 h; 2: With methanol; sulfuric acid 5 h; Heating;
参考文献
Sai, Hiroshi; Ogiku, Tsuyoshi; Ohmizu, Hiroshi; Ohtani, Akio
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1686 - 1693
622-42-4
硝基甲苯
+
624-49-7
富马酸二甲酯
→
反应条件
65859-90-7
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20°C; Michael addition/elimination; 1 h;
参考文献
Ballini, Roberto; Bosica, Giovanna; Mase, Aldo; Petrini, Marino
European Journal of Organic Chemistry, 2000 , # 16 p. 2927 - 2931
762-42-5
丁炔二酸二甲酯
+
103-80-0
氯化苯乙酰
→
反应条件
65859-90-7
+
65756-82-3
反应条件
1: With 1-methyl-1H-imidazole; N-ethyl-N,N-diisopropylamine in dichloromethane T=-10°C; 6 h; 2: With water in dichloromethane T=20°C; 48 h;
参考文献
Ding, Hanfeng; Ma, Cheng; Yang, Yewei; Wang, Yanguang
Organic Letters, 2005 , vol. 7, # 11 p. 2125 - 2127
186581-53-3
重氮甲烷
+
125702-14-9
→
反应条件
65859-90-7
反应条件
in diethyl ether T=20°C; Esterification; 1 h;
参考文献
Corral, Jose M. Miguel; Gordaliza, Marina; Castro, M. Angeles; Salinero, Miguel A.; Dorado, Jose M.; Feliciano, Arturo San
Synthesis, 2000 , # 1 p. 154 - 164
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