2-(乙酰氧基甲基)-6-叠氮基四氢-2H-吡喃-3,4,5-三基三乙酸酯合成路线 （共 6 条）
反应条件
1: With trimethylsilyl iodide in dichloromethane
0.5 h; Heating;
2: With tetra-N-butylammonium azide in dichloromethane
0.166667 h;
参考文献
Ying, Laiqiang; Gervay-Hague, Jacquelyn
Carbohydrate Research, 2003 , vol. 338, # 9 p. 835 - 841
反应条件
sodium azide in N,N-dimethyl-formamide
T=70°C; 13 h;
参考文献
Moyle, Peter M.; Olive, Colleen; Ho, Mei-Fong; Pandey, Manisha; Dyer, Joanne; Suhrbier, Andreas; Fujita, Yoshio; Toth, Istvan
Journal of Medicinal Chemistry, 2007 , vol. 50, # 19 p. 4721 - 4727
反应条件
sodium azide in N,N-dimethyl-formamide
T=80°C; 15 h;
参考文献
Cosgrove, Kelly L.; Bernhardt, Paul V.; Ross, Benjamin P.; McGeary, Ross P.
Australian Journal of Chemistry, 2006 , vol. 59, # 7 p. 473 - 476
反应条件
1: With trimethylsilylazide in 1,2-dichloro-ethane
T=20°C; 0.166667 h; Molecular sieve;
2: With copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=60°C; 0.0333333 h; Microwave irradiation;
参考文献
Sarkar, Swarbhanu; Dutta, Samrat; Sen, Asish Kumar
Synthesis, 2012 , vol. 44, # 7 p. 1079 - 1089
反应条件
sodium azide in water; acetone
T=20°C;
参考文献
Srivastava, Amrita; Varghese, Babu; Loganathan, Duraikkannu
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17720 - 17732
反应条件
1: HBr; acetic acid / CH2Cl2 / 5 h / 20 °C
2: 14 percent / NaN3 / dimethylformamide / 15 h / 80 °C
View Scheme
参考文献
Cosgrove, Kelly L.; Bernhardt, Paul V.; Ross, Benjamin P.; McGeary, Ross P.
Australian Journal of Chemistry, 2006 , vol. 59, # 7 p. 473 - 476
