反应条件
1: sodium chlorite; 2-methyl-but-2-ene; Dess-Martin periodane / dichloromethane; tert-butyl alcohol; aq. phosphate buffer / pH 7
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C
View Scheme
参考文献
Tremblay, Martin; Bonneau, Pierre; Bousquet, Yves; Deroy, Patrick; Duan, Jianmin; Duplessis, Martin; Gagnon, Alexandre; Garneau, Michel; Goudreau, Nathalie; Guse, Ingrid; Hucke, Oliver; Kawai, Stephen H.; Lemke, Christopher T.; Mason, Stephen W.; Simoneau, Bruno; Surprenant, Simon; Titolo, Steve; Yoakim, Christiane
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7512 - 7517