N,N,N',N',N'',N''-hexamethylphosphoric triamide; Bu3PI2 in diethyl ether
T=0°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Haynes, Richard K.; Holden, Malcolm
Australian Journal of Chemistry, 1982 , vol. 35, # 3 p. 517 - 524
Vizgert, R. V.; Korostylev, A. P.; Kru'tko, I. N.; Zen'kova, S. E.; Yakusheva, I. G.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 1 p. 120 - 124
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 1 p. 143 - 148
1: With diethylzinc; oxygen in n-heptane; dichloromethane
T=20°C; 14 h; Darkness;
2: With ammonium chloride in n-heptane; dichloromethane; water
regioselective reaction;
