N-(2-甲酰基苯基)-4-甲基苯磺酰胺合成路线 （共 24 条）
反应条件
piperidine in acetonitrile Friedlaender synthesis; 1 h; Reflux;
参考文献
Ukhin; Belov
Russian Chemical Bulletin, 2008 , vol. 57, # 2 p. 418 - 421
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h;
参考文献
Miyagi, Takashi; Hari, Yoshiyuki; Aoyama, Toyohiko
Tetrahedron Letters, 2004 , vol. 45, # 33 p. 6303 - 6305
反应条件
1: With triphenylphosphine in acetonitrile T=20°C; 4 h; Inert atmosphere; 2: With hydrogenchloride in water; acetonitrile 0.0833333 h; Inert atmosphere;
参考文献
Khong, San; Kwon, Ohyun
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8257 - 8267,11
反应条件
1.1: tetrahydrofuran / 3 h / Reflux; Inert atmosphere 1.2: 0.17 h / 20 °C / Inert atmosphere; Saturated solution 2.1: N-iodo-succinimide; 2-(dicyclohexylphosphino)-2',4',6'-triisopropylbiphenyl Au bis(trifluoromethylsulfonyl)imide / acetone / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Kothandaraman, Prasath; Lauw, Sherman Jun Liang; Chan, Philip Wai Hong
Tetrahedron, 2013 , vol. 69, # 35 p. 7471 - 7480
反应条件
1: 93 percent / propan-2-ol / 1.) boiling, 2.) 12 h 2: 94.4 percent / CuI / acetonitrile / 0.5 h / Heating 3: 95 percent / conc. H2SO4 / 2 h / 20 °C View Scheme
参考文献
Ukhin, L. Yu.; Komissarov, V. N.; Orlova, G. I.; Borodkin, G. S.; Lindeman, S. V.; et al.
Russian Chemical Bulletin, 1995 , vol. 44, # 11 p. 2142 - 2146
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 11 p. 2236 - 2240
反应条件
1: With triphenylphosphine in acetonitrile T=20°C; 10 h; Inert atmosphere; 2: With hydrogenchloride in water; acetonitrile 0.0833333 h; Inert atmosphere;
参考文献
Khong, San; Kwon, Ohyun
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8257 - 8267,11
反应条件
bromine; sodium acetate in water; acetic acid T=20°C; 4 h;
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
pyridinium chlorochromate in dichloromethane
3 h;
参考文献
Hewson, Alan T.; Hughes, Kevin; Richardson, Steward K.; Sharpe, David A.; Wadsworth, Alan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 6 p. 1565 - 1569
反应条件
pyridine in dichloromethane
T=20°C; 12 h;
参考文献
Varela-Fernandez, Alejandro; Varela, Jesus A.; Saa, Carlos
Synthesis (Germany), 2012 , vol. 44, # 21 art. no. SS-2012-Z0414-PSP, p. 3285 - 3295
反应条件
1: With pyridine in chloroform
T=20°C; 12 h;
2: With pyridinium chlorochromate in dichloromethane
参考文献
Rohlmann, Renate; Daniliuc, Constantin-Gabriel; Mancheno, Olga Garcia
Chemical Communications, 2013 , vol. 49, # 99 p. 11665 - 11667
