3,4-二氯异硫氰酸苯酯合成路线 （共 15 条）
反应条件
triethylamine in benzene T=10 - 20°C;
参考文献
Zakrzewski, Jerzy; Krawczyk, Maria
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1880 - 1903
参考文献
De Costa; Rice; Bowen; Thurkauf; Rothman; Band; Jacobson; Radesca; Contreras; Gray; Daly; Iyengar; Finn; Vazirani; Walker
Journal of Medicinal Chemistry, 1990 , vol. 33, # 11 p. 3100 - 3110
反应条件
potassium hydroxide T=20°C; 1.5 h; MillingGreen chemistry;
参考文献
Zhang, Ze; Wu, Hao-Hao; Tan, Ya-Jun
RSC Advances, 2013 , vol. 3, # 38 p. 16940 - 16944
反应条件
hydrogenchloride; toluene
参考文献
Journal of the American Chemical Society, , vol. 79, p. 1236,1242
Journal of Organic Chemistry, , vol. 24, p. 1676
反应条件
1: 3,4-dichloro-aniline With 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide T=20°C; 12 h; 2: bis(trichloromethyl) carbonate Reflux;
参考文献
Chemical Biology and Drug Design, , vol. 76, # 1 p. 25 - 33
参考文献
Angewandte Chemie, , vol. 78, p. 748 - 749
反应条件
1: 20 - 25 °C 2: 125 - 130 °C View Scheme
参考文献
Angewandte Chemie, , vol. 78, p. 748 - 749
反应条件
in benzene T=0 - 20°C;
参考文献
Zakrzewski, Jerzy; Krawczyk, Maria
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1880 - 1903
参考文献
BRISTOL-MYERS SQUIBB COMPANY; KING, Dalton; OLSON, Richard E.; MACOR, John E.; ISLAM, Imadul; THANGATHIRUPATHY, Srinivasan; WARRIER, Jayakumar Sankara
Patent: WO2013/49119 A1, 2013 ;
Location in patent: Page/Page column 253 ;
反应条件
1: toluene 2: aq. HCl View Scheme
参考文献
Chupp,J.P.; Weiss,E.R.
Journal of Organic Chemistry, 1968 , vol. 33, p. 2357 - 2361
