1-羟基-2-异丙基-8-甲基-3,4-菲二酮合成路线 （共 7 条）
反应条件
1: 2.) DDQ / 1.) AcOH, reflux
2: K2CO3 / tetrahydrofuran; H2O
View Scheme
参考文献
Zhang, Zhao-Rong; Flachsmann, Felix; Moghaddam, Firouz Matloubi; Rueedi, Peter
Tetrahedron Letters, 1994 , vol. 35, # 14 p. 2153 - 2156
反应条件
1: 2.) DDQ / 1.) AcOH, reflux
2: K2CO3 / tetrahydrofuran; H2O
View Scheme
参考文献
Zhang, Zhao-Rong; Flachsmann, Felix; Moghaddam, Firouz Matloubi; Rueedi, Peter
Tetrahedron Letters, 1994 , vol. 35, # 14 p. 2153 - 2156
反应条件
potassium carbonate in tetrahydrofuran; water
参考文献
Zhang, Zhao-Rong; Flachsmann, Felix; Moghaddam, Firouz Matloubi; Rueedi, Peter
Tetrahedron Letters, 1994 , vol. 35, # 14 p. 2153 - 2156
反应条件
1: 1.) LiHMDS, TFEA, 2.) MsN3, Et3N / 2.) H2O, CH3CN
2: 1,2-dichloro-ethane / Irradiation; 1.) r.t., 2.) 90 deg C
3: n-Bu4NF, O2 / tetrahydrofuran / -78 deg C to r.t.
View Scheme
参考文献
Danheiser, Rick L.; Casebier, David S.; Loebach, Jennifer L.
Tetrahedron Letters, 1992 , vol. 33, # 9 p. 1149 - 1152
反应条件
1: 1,2-dichloro-ethane / Irradiation; 1.) r.t., 2.) 90 deg C
2: n-Bu4NF, O2 / tetrahydrofuran / -78 deg C to r.t.
View Scheme
参考文献
Danheiser, Rick L.; Casebier, David S.; Loebach, Jennifer L.
Tetrahedron Letters, 1992 , vol. 33, # 9 p. 1149 - 1152
反应条件
2: acetic acid
View Scheme
参考文献
Baillie,A.C.; Thomson,R.H.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 48 - 52
参考文献
Baillie,A.C.; Thomson,R.H.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 48 - 52
