1-硬脂酰-2-花生酰-SN-甘油合成路线 （共 12 条）
反应条件
pyrrole; trifluoroacetic acid in dichloromethane T=20°C; 1 h;
参考文献
Kubiak, Robert J.; Bruzik, Karol S.
Journal of Organic Chemistry, 2003 , vol. 68, # 3 p. 960 - 968
反应条件
methanol; anhydrous iron chloride in dichloromethane T=20°C; 8.91667 h;
参考文献
Anderson, Regan J.; Osborne, Shona L.; Meunier, Frederic A.; Painter, Gavin F.
Journal of Organic Chemistry, 2010 , vol. 75, # 11 p. 3541 - 3551
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; acetic acid T=0°C; 1 h;
参考文献
Greimel, Peter; Ito, Yukishige
Tetrahedron Letters, 2008 , vol. 49, # 22 p. 3562 - 3566
反应条件
dichloro-acetic acid; pyrrole in dichloromethane 0.0833333 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 14 p. 2539 - 2542
反应条件
dichloro-acetic acid; pyrrole in dichloromethane 0.0833333 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 38, # 14 p. 2539 - 2542
反应条件
1: 76 percent / glacial AcOH / 20 - 35 °C / 15 Torr 2: 1.794 g / 1-methylimidazole; 2,6-Cl2C6H3COCl / CH2Cl2 / 1.33 h / 20 °C 3: Cl2CHCO2H; pyrrole / CH2Cl2 / 0.08 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 2 p. 192 - 205
反应条件
1: CF3CO2H; CF3CH2OH; B(OEt)2 / 5 h / 20 °C 2: 76 percent / glacial AcOH / 20 - 35 °C / 15 Torr 3: 1.794 g / 1-methylimidazole; 2,6-Cl2C6H3COCl / CH2Cl2 / 1.33 h / 20 °C 4: Cl2CHCO2H; pyrrole / CH2Cl2 / 0.08 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 2 p. 192 - 205
反应条件
1: 1.794 g / 1-methylimidazole; 2,6-Cl2C6H3COCl / CH2Cl2 / 1.33 h / 20 °C 2: Cl2CHCO2H; pyrrole / CH2Cl2 / 0.08 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 2 p. 192 - 205
反应条件
1: 2,6-dichlorobenzoyl chloride, 1-methylimidazole / CH2Cl2 / Ambient temperature 2: Cl2CHCO2H, pyrrole / CH2Cl2 / 0.08 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 14 p. 2539 - 2542
反应条件
1: Et3N, DMAP / CH2Cl2 / 0.83 h / 0 deg C to RT 2: CF3COOH, CF3CH2OH, B(OEt)3 / 5.5 h / Ambient temperature 3: acetic acid / 15 Torr / RT to < 30 deg C 4: 2,6-dichlorobenzoyl chloride, 1-methylimidazole / CH2Cl2 / Ambient temperature 5: Cl2CHCO2H, pyrrole / CH2Cl2 / 0.08 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 14 p. 2539 - 2542
