1-硬脂酰-2-花生酰-SN-甘油合成路线 (共 12 条)
反应条件
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0.25 h / 20 °C / |Inert atmosphere 1.2: 20 °C / |Inert atmosphere 2.1: FeCl3·6H2O / dichloromethane; methanol / 0.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 24 p. 6330 - 6334
Angew. Chem., , vol. 125, # 24 p. 6455 - 6459,5
反应条件
1.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 95 °C / |Inert atmosphere 2.1: iodine; sodium carbonate / tetrahydrofuran; water / 5 h / 20 °C / |Inert atmosphere 3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0.25 h / 20 °C / |Inert atmosphere 3.2: 20 °C / |Inert atmosphere 4.1: FeCl3·6H2O / dichloromethane; methanol / 0.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 24 p. 6330 - 6334
Angew. Chem., , vol. 125, # 24 p. 6455 - 6459,5