lithium aluminium tetrahydride in diethyl ether

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '17084631', constants.ctx, '0')">[Rh(1,5-cyclooctadienyl)(μ-OCH₃)]₂</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '957171', constants.ctx, '0')">tri-cyclo-hexyl-phosphine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '506008', constants.ctx, '0')">dimethyl sulfoxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=25&deg;C;&nbsp;6&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342958', constants.ctx, '0')">tin</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1209232', constants.ctx, '0')">chloro-trimethyl-silane</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=20&deg;C;&nbsp;Addition;&nbsp;1.5&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <br />&nbsp;1) hexane, THF, -70 deg C, 1 h, 2) THF, -70 deg C up to r.t.;&nbsp;&nbsp;Yield given. Multistep reaction;&nbsp;<br /> &nbsp;