反应条件
in tetrahydrofuran byproducts: NaCl; Ar atmosphere, filtration of metal complex soln. through Kieselgur to a tube containing the solid ligand at 20°C; filtration (Kieselgur), evapn. to dryness, dissolution (THF), chromy. (silica gel, elution of byproducts with Et2O, elution of main product withTHF), removement of solvent (vacuum); elem. anal.;
参考文献
Kircher, Peter; Huttner, Gottfried; Heinze, Katja; Schiemenz, Berthold; Zsolnai, Laszlo; Buechner, Michael; Driess, Alexander
European Journal of Inorganic Chemistry, 1998 , # 6 p. 703 - 720