反应条件
1: methylmagnesium bromide With titanium(IV) isopropylate; bis[2-(N,N-dimethylamino)ethyl] ether; (S)-(minus;)-1,1'-bi-2-naphthol in tetrahydrofuran; tert-butyl methyl ether T=20°C; Inert atmosphereCooling with ice; 2: 1-naphthaldehyde in tetrahydrofuran; tert-butyl methyl ether T=20°C; Inert atmosphereCooling with ice; optical yield given as percent eeenantioselective reaction;
参考文献
Liu, Yi; Da, Chao-Shan; Yu, Sheng-Li; Yin, Xiao-Gang; Wang, Jun-Rui; Fan, Xin-Yuan; Li, Wei-Ping; Wang, Rui
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6869 - 6878
