反应条件
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere 2: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 20 - 100 °C / Inert atmosphere 3: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice 4: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926