二苯基碘三氟甲烷磺酸盐合成路线 (共 201 条)
反应条件
sodium t-butanolate T=110°C; 10 h; under air;
参考文献
Wen, Jun; Zhang, Ruo-Yi; Chen, Shan-Yong; Zhang, Ji; Yu, Xiao-Qi
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 766 - 771
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Organic Letters, , vol. 15, # 1 p. 188 - 191
反应条件
1: 4-methoxyphenyl magnesium bromide With (DABCO)*(SO2)2 in tetrahydrofuran T=-40°C; 1 h; Inert atmosphere; 2: Diphenyliodonium triflate in N,N-dimethyl-formamide T=120°C; 5 h; Inert atmosphereMicrowave irradiation;
参考文献
Deeming, Alex S.; Russell, Claire J.; Hennessy, Alan J.; Willis, Michael C.
Organic Letters, 2014 , vol. 16, # 1 p. 150 - 153
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 19 p. 4972 - 4975
反应条件
1: 2-iodophenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: Diphenyliodonium triflate in tetrahydrofuran T=40°C; 1 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
1: 3-trifluoromethyl-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: Diphenyliodonium triflate in tetrahydrofuran T=40°C; 0.5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
sodium hydroxide in water T=20 - 60°C; 3 h;
参考文献
Organic Letters, , vol. 15, # 23 p. 6070 - 6073