二苯基碘三氟甲烷磺酸盐合成路线 （共 201 条）
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile
T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique; TimeTemperatureReagent/catalystConcentration;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile
T=25°C; 12 h; Schlenk techniqueInert atmosphereIrradiation;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
反应条件
potassium tert-butylate in toluene
T=0°C; 1.25 h; Reflux;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid
T=100°C; 24 h; Overall yield = 96 percent; Overall yield = 43.5 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid
T=100°C; 24 h; Overall yield = 79 percent; Overall yield = 35.9 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
triethylamine; copper(l) chloride in dichloromethane
T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
反应条件
in N,N-dimethyl-formamide
T=100°C; 0.333333 h; Microwave irradiation;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
European Journal of Organic Chemistry, 2012 , # 35 p. 6852 - 6855
反应条件
1: ethyl 2-oxo-cyclopentanecarboxylate With N1-benzyl-O-benzoylcinchonidinium chloride; potassium hydroxide in toluene
T=20°C; 1 h;
2: Diphenyliodonium triflate in toluene
T=20°C; Cooling with acetone-dry ice;
参考文献
Norrby, Per-Ola; Petersen, Tue B.; Bielawski, Marcin; Olofsson, Berit
Chemistry - A European Journal, 2010 , vol. 16, # 28 p. 8251 - 8254
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid
T=100°C; 24 h; Overall yield = 79 percent; Overall yield = 41.3 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
copper(II) bis(trifluoromethanesulfonate); sodium salt of phosphorous acid in toluene
T=100°C; 15 h; Inert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Kuriyama, Masami; Hamaguchi, Norihisa; Onomura, Osamu
Chemistry - A European Journal, 2012 , vol. 18, # 6 p. 1591 - 1594
