二苯基碘三氟甲烷磺酸盐合成路线 （共 201 条）
反应条件
1: m-hydroxynitrobenzene With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: Diphenyliodonium triflate in tetrahydrofuran
T=40°C; 0.5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
1: p-hydroxyacetanilide With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: Diphenyliodonium triflate in tetrahydrofuran
T=40°C; 2.5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
in N,N-dimethyl-formamide
T=100°C; 22 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Dellacqua, Monica; Fenner, Sabine; Vicente, Ruben; Sandmann, Rene
Organic Letters, 2011 , vol. 13, # 9 p. 2358 - 2360
反应条件
2,6-di-tert-butyl-pyridine; copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=35°C; 14 h;
参考文献
Phipps, Robert J.; Grimster, Neil P.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8172 - 8174
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid
T=100°C; 24 h;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); trifluoroacetic acid
T=100°C; 24 h; Overall yield = 96 percent; Overall yield = 43.5 mg;
参考文献
Storr, Thomas E.; Greaney, Michael F.
Organic Letters, 2013 , vol. 15, # 6 p. 1410 - 1413
反应条件
in N,N-dimethyl-formamide
T=90°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 19 p. 4972 - 4975
反应条件
sodium hydroxide in water
T=20 - 50°C; 6 h;
参考文献
Lindstedt, Erik; Ghosh, Raju; Olofsson, Berit
Organic Letters, 2013 , vol. 15, # 23 p. 6070 - 6073
反应条件
potassium thiocyanate in neat (no solvent)
T=120°C; 0.333333 h; Microwave irradiation; regioselective reaction;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
European Journal of Organic Chemistry, 2012 , # 35 p. 6852 - 6855
反应条件
1: n-hexyl selenocyanate With ethanol in N,N-dimethyl-formamide
T=20°C;
2: With sodium tetrahydroborate in N,N-dimethyl-formamide
3: Diphenyliodonium triflate in N,N-dimethyl-formamide
T=20°C; 1 h; Further stages.;
参考文献
Krief, Alain; Dumont, Willy; Robert, Michael
Synlett, 2006 , # 16 p. 2601 - 2604
