4',5,7,8-四甲氧基黄酮合成路线 （共 21 条）
反应条件
hydrogen iodide; acetic anhydride
参考文献
Oliverio et al.
Gazzetta Chimica Italiana, 1948 , vol. 78, p. 363,370
反应条件
1: H2 / Pd-C
2: AlCl3 / nitrobenzene / Ambient temperature
3: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
1: (CF3CO)2O / benzene / 4 h / Ambient temperature
2: KOH / pyridine / 0.33 h / 110 °C
3: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
4: H2 / Pd-C
5: AlCl3 / nitrobenzene / Ambient temperature
6: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
1: (CF3CO)2O / benzene / 4 h / Ambient temperature
2: KOH / pyridine / 0.33 h / 110 °C
3: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
4: H2 / Pd-C
5: AlCl3 / nitrobenzene / Ambient temperature
6: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
1: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
2: H2 / Pd-C
3: AlCl3 / nitrobenzene / Ambient temperature
4: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
1: KOH / pyridine / 0.33 h / 110 °C
2: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
3: H2 / Pd-C
4: AlCl3 / nitrobenzene / Ambient temperature
5: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
sodium 4-methoxyphenylacetate
T=180°C;
参考文献
Wessely; Kallab
Monatshefte fuer Chemie, 1932 , vol. 60, p. 26,30
Full Text Show Details
Hattori
Acta Phytochimica, 1930 , vol. 5, p. 219,230, 231
反应条件
1: AlCl3 / nitrobenzene / Ambient temperature
2: K2CO3 / acetone / 5 h / Heating
View Scheme
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
potassium carbonate in acetone
5 h; Heating;
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
反应条件
potassium carbonate in acetone
5 h; Heating;
参考文献
Iinuma; Matsuura; Kurogochi; Tanaka
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 3 p. 717 - 722
