3-甲基-1,2-苄异恶唑-6-醇合成路线 (共 8 条)
反应条件
triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 0.0166667 h;
参考文献
Tetrahedron Letters, , vol. 47, # 47 p. 8247 - 8250
反应条件
potassium hydroxide in methanol; water
反应条件
T=125°C; P=0.1 Torr; 1 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 7 p. 571 - 575
反应条件
1: 1) 40percent KOH 2) NH2OH*HCl / 1) H2O 2) 4h 2: Heating 3: 1 h / 125 °C / 0.1 Torr View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 7 p. 571 - 575
反应条件
potassium carbonate; potassium iodide in acetone
Heating;
参考文献
Sahasrabudhe, A. B.; Kamath, S. V.; Bapat, B. V.; Bhawal, B. M.; Kulkarni, Sheshagiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1266 - 1267
反应条件
1: 9 g / conc. nitric acid, acetic acid / 0.25 h / T<10 deg C
2: 100 percent / hydrogen, HCl / 10percent Pd-charcoal / methanol / 2 h / 760 Torr
View Scheme
参考文献
Rao, E. V. S. Bhushana; Kumari, S. Subhadra; Rao, K. S. R. Krishna Mohan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 366 - 367
反应条件
potassium carbonate; potassium iodide in acetone
Heating;
参考文献
Sahasrabudhe, A. B.; Kamath, S. V.; Bapat, B. V.; Bhawal, B. M.; Kulkarni, Sheshagiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 12 p. 1266 - 1267
反应条件
1: 55 percent / aq. KOH / 12 h / Heating
View Scheme
参考文献
Kutty, N. Gopalan; Bhat, A. R.
Journal of the Indian Chemical Society, 1993 , vol. 70, # 2 p. 178 - 179