1-(呋喃-2-基)-2-丙醇合成路线 (共 4 条)
反应条件
aluminum oxide; pyridinium chlorochromate in dichloromethane 24 h;
参考文献
Fogagnolo, Marco; Giovannini, Pier Paolo; Guerrini, Alessandra; Medici, Alessandro; Pedrini, Paola; Colombi, Nicola
Tetrahedron Asymmetry, 1998 , vol. 9, # 13 p. 2317 - 2327
反应条件
1: furan With n-butyllithium in diethyl ether; hexane
T=10 - 20°C;
2: methyloxirane in diethyl ether; hexane
T=20°C; 3 h;
参考文献
Loiseau, Francois; Simone, Jean-Mary; Carcache, David; Bobal, Pavel; Neier, Reinhard
Monatshefte fur Chemie, 2007 , vol. 138, # 2 p. 121 - 129
反应条件
1: 2-bromofuran With n-butyllithium in tetrahydrofuran
T=-30°C; 0.5 h;
2: methyloxirane in tetrahydrofuran
T=20°C; 1 h; Further stages.;
参考文献
Allan; Carnell
Journal of Organic Chemistry, 2001 , vol. 66, # 19 p. 6495 - 6497
反应条件
n-butyllithium; ammonium chloride; methyloxirane in tetrahydrofuran
参考文献
Baxter, Andrew; Brough, Stephen; Faull, Alan; Johnstone, Craig; McInally, Thomas
Patent: US2002/107252 A1, 2002 ;