1-(3,4-二甲氧基苯基)-1-戊酮合成路线 （共 8 条）
反应条件
1: 21 percent / Zn; aq. HCl / toluene / 72 h / Heating 2: 39 percent / Me3SiI / acetonitrile / 60 h / 20 °C View Scheme
参考文献
Kraft, Philip; Eichenberger, Walter
European Journal of Organic Chemistry, 2003 , # 19 p. 3735 - 3743
反应条件
hydrogenchloride; zinc in toluene Clemmensen reduction; 72 h; Heating;
参考文献
Kraft, Philip; Eichenberger, Walter
European Journal of Organic Chemistry, 2003 , # 19 p. 3735 - 3743
反应条件
1: in tetrahydrofuran
T=0°C; Green chemistry;
2: With [bis(acetoxy)iodo]benzene
T=0 - 20°C; Green chemistry;
参考文献
Sagara, Prateep Singh; Chebolu, Rajesh; Bahuguna, Ashish; Ravikumar
RSC Advances, 2014 , vol. 4, # 29 p. 15011 - 15013
反应条件
sodium hydrogencarbonate; lithium diisopropyl amide in water; ethyl acetate
参考文献
Celgene Corporation
Patent: US6429221 B1, 2002 ;
反应条件
gallium(III) chloride; silver perchlorate in dichloromethane
6 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Ohno, Takashi; Nishimura, Takashi; Suda, Shinji; Kobayashi, Shu
Chemistry Letters, 1991 , # 6 p. 1059 - 1062
Title/Abstract Full Text Show Details
Harada; Ohno; Kobayashi; Mukaiyama
Synthesis, 1991 , # 12 p. 1216 - 1220
反应条件
tetrachlorosilane; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane
20 h; Ambient temperature;
参考文献
Suzuki; Kitagawa; Mukaiyama
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 12 p. 3729 - 3734
反应条件
tetrachlorosilane; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane
24 h; Ambient temperature;
参考文献
Suzuki; Kitagawa; Mukaiyama
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 12 p. 3729 - 3734
反应条件
diphenylboryl triflate in dichloromethane
24 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Nagaoka, Hitoshi; Ohshima, Masahiro; Murakami, Masahiro
Chemistry Letters, 1986 , p. 165 - 168
