1,1-二氯-2-碘-1,2,2-三氟乙烷合成路线 (共 13 条)
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=70°C; 21 h;
参考文献
Cherstkov, V. F.; Postovoi, S. A.; Lantseva, D. T.; Sterlin, S. R.; Zeifman, Yu. V.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2508 - 2511
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2740 - 2743
反应条件
1: With zinc in ethyl acetate
T=20°C; 41 h;
2: With zinc in isopropyl alcohol
T=80°C; 2 h;
参考文献
Karimova; Glazkov; Ignatenko; Mysova
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2336 - 2337
反应条件
zinc in ethyl acetate
T=20°C; 41 h; Title compound not separated from byproducts;
参考文献
Karimova; Glazkov; Ignatenko; Mysova
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2336 - 2337